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    • ⇒ ICES: International Council for the Exploration of the Sea
    • ICES Techniques in Marine Environmental Sciences
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    •   Repository OceanBestPractices
    • ⇒ ICES: International Council for the Exploration of the Sea
    • ICES Techniques in Marine Environmental Sciences
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    Chlorobiphenyls in marine sediments: Guidelines for determination.

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    Date
    1998
    Author
    Smedes, F.
    de Boer, J.
    Status
    Published
    Pages
    24pp.
    
    Metadata
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    Abstract
    The analysis of chlorinated biphenyls in sediments generally includes extraction with organic solvents, clean-up, removal of sulphur, colullUl fractionation and gas chromatographic separation, mostly with electron capture detection. All of the steps in the procedure are susceptible to insufficient recovery and/or contamination. Different methods applied to each of these steps are discussed with their advantages and disadvantages. Where possible, quality control procedures are recommended in order to check the method's performance. Gas chromatographic conditions are discussed with regard to injection, separation, detection and system performance. In addition, the quality control aspects relating to calibrants, extraction, and clean-up are considered. These guidelines are intended to encourage and assist analytical chemists to critically (re)consider their methods and to improve their procedures and/or the associated quality control measures, where necessary......
    Resource URL
    http://ices.dk/publications/library/
    Publisher
    International Council for the Exploration of the Sea (ICES)
    Copenhagen, Denmark
    Series;Nr
    ICES Techniques in Marine Environmental Sciences; 21
    Document Language
    en
    Sustainable Development Goals (SDG)
    14.1
    Best Practice Type
    Standard Operating Procedure
    Guide
    ISSN
    0903–2606
    Citation
    Smedes, F. and de Boer, J. (1998) Chlorobiphenyls in marine sediments: Guidelines for determination. ICES Techniques in Marine Environmental Sciences, No. 21, 24pp. DOI: http://dx.doi.org/10.25607/OBP-270
    URI
    http://hdl.handle.net/11329/713
    http://dx.doi.org/10.25607/OBP-270
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    • ICES Techniques in Marine Environmental Sciences [59]

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